合成した錯体の熱分解温度は熱重量示差熱測定（TG/DTA）によって決定

合成した錯体の熱分解温度は熱重量示差熱測定（TG/DTA）によって決定した。
なお5 %重量減少温度を熱分解温度として定義した。また偏光顕微鏡（POM）
観察および示差走査熱量測定（DSC）により相転移挙動を観察した。各錯体の
TG/DTA 曲線を図2-3，DSC 曲線を図2-4，偏光顕微鏡写真を図2-5 に示す。ま
たこれらの測定により決定した各錯体の相転移温度を表2-3 と図2-6 に，エンタ
ルピー変化とエントロピー変化を表2-4 に示す。

ผลลัพธ์ (อังกฤษ) 1:

Thermal decomposition of synthesized complexes determined by Thermogravimetry shows difference between heat (TG/DTA).However 5% weight decrease temperature was defined as the pyrolysis temperature. It's also polarizing microscope (POM)Observations and differential scanning calorimetry (DSC) phase transition behaviours observed. Each complexTG/DTA curve DSC curve, shown in Figure 2-3 shown in Figure 2-5 polarization microscope, shown in Figure 2-4. .This is from of each complex was determined by measuring the phase transition temperature table 2-3 and 2-6 in, entertainmentRupees and entropy changes shown in table 2-4.

ผลลัพธ์ (อังกฤษ) 2:

Thermal decomposition temperature of the synthesized complexes was determined by thermogravimetric differential thermal measurement (TG / DTA).
It should be noted that the 5% weight reduction temperature I was defined as the thermal decomposition temperature. The polarized light microscopy (POM)
we observed a phase transition behavior by observation and differential scanning calorimetry (DSC). Of each complex
a TG / DTA curve Figure 2-3, Figure 2-4, it is shown in Figure 2-5 a polarizing microscope photograph the DSC curve. Or
the phase transition temperature of each complex was determined by these measurements was to Table 2-3 and Figure 2-6, Enta
I show the rupee change and entropy change in Table 2-4.

ผลลัพธ์ (อังกฤษ) 3:

Thermogravimetric and differential thermal pyrolysis temperature measurement of the complex was synthesized, and DTA TG) was determined by. At 5 in the thermal decomposition temperature and the temperature decrease in weight. Polarizing microscopy and differential scanning calorimetry (DSC observation and POM (HTS) were observed by the phase transition behavior. Fig. 2 or 3. ， TG DTA curve of the complex curve DSC 2-4 in Fig. 2 ， in polarizing microscope. Based on these measurements into it. To determine the phase transition temperatures of the complexes and the table 6 in Fig. 2 ， entropy and enthalpy change at shown in Table 2.